STEPS IN MAKING LIQUID SOAP

REQUIRED CHEMICALS NEEDED AND THEIR QUANTITIES

  1. Nitrosol (or Antisol)…….……… 1/8kg (i.e 125g).
  2. Caustic Soda…………………..……1/16kg (i.e 62.5g)
  3. Soda Ash (Sodium carbonate) ,,..1/8 Kg
  4. SLS (Sodium Lauryl Sulphate) ….1/8kg
  5. Sulphonic Acid………………..……..1 ½ Ltr
  6. STPP……………………………….… 1/16Kg
  7. Texapon ………………………….…1/8kg
  8. Foam Booster………………………1/6 Ltr
  9. Formalin………………………………10Cl
  10. Colour (As desired)
  11. Glycerine (Optional)
  12. Perfume (As desired)
  13. Vitamin E (Optional)

DESCRIPTION AND FUNCTIONS OF CONSTITUENTS USED FOR THE PRODUCTION OF LIQUID SOAP

Water:

Water is the main solvent needed for the process to dissolve the various ingredients and also during fermentation phase. It is very essential in the production of liquid soap.

Nitrosol/Antisol:

Nitrosol

This serves as a thickener in the production of the liquid soap. It comes as a whitish substance and has the texture of a powdered milk. Nitrosol will dissolve immediately in water, but Antisol takes longer time to dissolve in water.

Caustic Soda:

Caustic Soda

It is whitish crystalline substances that looks much like a sample of granulated sugar. It forms a strong base when dissolved in water and can be corrosive if in contact with the skin. It is an essential ingredient in the soap making process. This is the stain or dirt removing agent in the liquid soap.

Soda Ash (Sodium carbonate):

Soda Ash

This is also a whitish substance but with much coarse grains, it serves to regulate the concentration of the Caustic Soda which ordinarily is corrosive to the skin. It helps to neutralize it.

SLS (Sodium Lauryl Sulphate):

SLS

The SLS looks like rice grains and it’s whitish in colour too. It is a surfactant which helps to lower the surface tension of the aqueous solution. It is the main active foaming agent.

Texapon:

Texapon

The Taxapon is a pasty and jellylike substance, it also functions as a foaming agent and serves as foaming booster too. Many liquid soap producers don’t use Texapon and SLS together in same production; reason because both perform almost same function. They go with just one.

Sulphonic Acid:

Sulphonic Acid

This is a dark looking liquid substance. It serves to boost the performance of the SLS, it is also a foaming and cleaning agent. Please the word spells S-U-L-P-H-O-N-I-C and not S-U-L-P-H-U-R-I-C. The latter is very strong acid and can be very corrosive. please beware.

STPP (Sodium Tripolyphosphate):

STPP

STPP is a sodium salt of triphosphoric acid. It has the appearance of white crystal powder and looks very much like a table salt. It is a strong cleaning agent too and helps the SLS to work on its full potential.

Forming Booster:

Foaming booster

This also comes in liquid form and has transparent looks. As the name implies, it makes the liquid soap to foam very well.

Formalin:

The preservative agent. It should be used if the soap is to be stored for a long time like six months, especially if one is producing for commercial purposes. Please you can do without this chemical. It is very harmful if abused, it can cause CANCER.

Colour:

This normally comes as a powder and should be diluted with water before adding to the soap mixture. The colour adds beauty to the finished product. Most producers go with green colour.

Glycerine:

Usually helps your skin to remain hydrated and soft after using the soap.

Perfume:

This gives your soap a sweet fragrance. Most people prefer the lemon, pineapple, ambipur. lavender or strawberry fragrance in their production.

Vitamin E:

Offers a great deal of protection to the skin. E.g from damage, wrinkles etc.

YOU MAY NEED

  1. A big mixing bowl
  2. Containers
  3. Wooden spoon or stick for stirring
  4. A pair of Scissors
  5. Spoon
  6. Measurement bowl or container
  7. Hand glove
  8. Nose mask
  9. Rubber gloves

METHODOLOGY FOR LIQUID SOAP

A great deal of patience is required when stirring the constituent mixturs.

For smaller volume production, eg 8litres or 10litres. follow same process but work on your ratios. The vendors selling these chemicals usually sell them  already measured according to the volume of liquid soap to be produced. Just tell them how much volume you want to produce and they will give you the quantity of chemicals you require. It is advisable to start with small volume and grow big later. Measure out about 20 litres of water; follow the steps below:

  1. Ferment the Caustic Soda before production process by dissolving with 1 litre of water and allowing for 24 hours or overnight. Please keep all chemicals out of reach of children. Caustic soda is corrosive to the skin.
  2. Dissolve the Soda Ash as above (i.e with 1 litre of water and keep overnight for fermentation to take place)
  3. Dissolve the Nitrosol with 10 litres of water in a bigger mixing bowl just before production. In case you want to opt for Antisol in preference to Nitrosol, dissolve in same amount of water and let it stay for at least 24-48 hours before production. Note: this should be properly dissolved and will look like ‘starchy solution’ at the end.
  4. Dissolve the SLS (Sodium Lauryl Sulphate) in 1 litre of water to produce a clear solution before production; keep it aside. This should be done at least one hour  before production. If you want it to dissolve well, dissolve in water and leave over night.
  5. Dissolve the STPP (Sodium Tripolyphosphate) in 1 litre of water before production and keep aside too. (Some people don’t use STPP for whatever reasons best known to them)
  6. Mix the Texapon and Sulphonic Acid together. Mix very well and dissolve further with 2 litres of water. Stirring should be done gently until mixture is well dissolved and homogenous. Note that this particular step is exothermic process; meaning that heat will be generated if you do it well.
  7. Dissolve the powdered colour with small quantity of water and keep aside.
  8. Gently pour the dissolved mixture of Sulponic Acid and Texapon into the mixing bowl containing dissolved Nitrosol(or Antisol}. Stir very well and gently until mixture becomes homogenous. You need patience here.
  9. Add the dissolved Caustic Soda into the mixing bowl above and stir very well.
  10. Add the dissolved Soda Ash next and stir very well until even.
  11. Next, add the STPP and stir properly
  12. Add the Dissolved SLS and stir more.
  13. Add Foam Booster to make it foam very well.
  14. Add your Formalin and keep stirring
  15. Vitamin E and Glycerine can be added at this point. Dont forget to stir and stir.
  16. Finally, allow the lather formed to disappear, then add the dissolved colour and perfume, and stir properly.
  17. Now add the remaining  water. Do this gradually, small quantity at a time, stir each time and pay close watch on the thickness until the desired is attained.

Note: Following this order is very important; if otherwise, you may end up producing something you may not like. Some people also believe that the SLS and Texapon should not be used together, that it’s either one uses Texapon alone or SLS alone, but not the two. Like I mentioned earlier, there are diverse methods of production and one should stick to whichever that works for him. For me, I use the two.

More so, the manner one mixes the SLS, Texapon. STPP, Sulphonic and Foaming Booster doesn’t really matter. The important thing is that the Caustic Soda goes into the mixing bowl containing the Nitrosol/Antisol first, then followed by Soda Ash. Then these (SLS/Texapon. STPP, Sulphonic and Foaming Booster), Vitamin E and Glycerine, and Finally Colour and Perfume.

A GOOD LIQUID SOAP HAS THE FOLLOWING QUALITIES

  1. Liquid soap is expected to foam very well.
  2. It must have a sweet fragrance.
  3. The colour must be appealing.
  4. Must be durable.
  5. Must not cause any form of irritation to the skin.

PRECAUTIONARY MEASURES AND SAFETY REQUIREMENTS

  1. Wear rubber gloves
  2. Use nose mask
  3. Carryout production in a well-ventilated environment with good illumination.
  4. In case of chemical splash to the face or delicate part of the body, wash very well with plenty water and see a physician as soon as you can.
  5. Keep all chemicals out of reach of children.
  6. Never taste any chemical with the tongue.
  7. Wear your apron or other protective clothing before you commence production.
  8. Most importantly, use your head. Don’t play with chemicals please.